slightly into the jar. Either tie in place or secure with a rubber band.
Pour about 1 fluid ounce of concentrated sulfuric acid into a small glass jar with a glass stopper and seal tightly.
d. Application .
Place the jar with the rubber membrane at the desired target. Pile the material to be ignited around this jar so that when the flames issue from the jar, they will ignite the incendiary materials. Do not put any of this igniter material on the rubber membrane. Pour the 1 fluid ounce of concentrated sulfuric acid onto the rubber membrane. When the acid penetrates the rubber and drips onto the igniter mix, a chemical reaction occurs and combustion results.
The time delay of this device depends on the kind and thickness of rubber used, and on the ambient temperature. Test a similar device before actual use on the target.
Using a thin rubber membrane such as a condom at a temperature of 77° F., a delay time of 15 to 20 minutes is normal. This same delay when tested at 40° F. may take as long as eight hours to penetrate the rubber membrane. Do not use this delay at temperatures below 40° F.
Another simple method of using this type of delay is to first fill a small jar half full of concentrated sulfuric acid. Tie or tape a rubber membrane over the open end of the jar. BE SURE NO ACID CAN LEAK OUT. Place the bottle on its side, on top of a small pile of igniter material which will ignite on contact with the acid. When the acid penetrates the membrane, combustion will occur as before. If thicker rubber is used, stretch the rubber tightly over the mouth of the jar. This will decrease the delay time because the acid will attack the stretched rubber more effectively.
A rubber glove may also be used as a membrane for this delay. Pour some concentrated sulfuric acid into the glove and suspend the glove over a pile of igniter material. When the acid eats through the glove, it will drip onto the igniter and start a fire. A rubber glove will give a longer delay time than a condom because the material is thicker.
The rubber membranes for use in this delay must be without pin holes or other imperfections. The sulfuric acid must be concentrated. If only battery-grade sulfuric acid is available, it must be concentrated before use to a specific gravity of 1.835 by heating it in an enameled, heat-resistant glass or porcelain pot until dense, white fumes appear. See paragraph 0103 for details.
0404. PAPER DIAPHRAGM (SULFURIC ACID)
a. Description.
This device consists of a half-full jar of concentrated sulfuric acid, and a paper diaphragm. The paper diaphragm is a piece of paper tied securely over the mouth of the jar. When the jar is placed on its side, the acid soaks through or corrodes the paper. The acid then contacts the igniter material and causes it to burts into flames. This delay can be used for initiating the following igniters listed in chapter 3: Sugar-Chlorate (0201), Fire Fudge (0202), SugarâSodium Peroxide (0203), Aluminum PowderâSodium Peroxide (0204), Match Head (0205), Silver NitrateâMagnesium Powder (0208).
b. Material and Equipment
Wide-mouthed jar.
Sulfuric acid (concentrated).
Paper.
String.
c. Preparation. Remove the cap from a wide-mouthed jar Fill about half-full with concentrated sulfuric acid. Tie the paper securely over the mouth of the jar.
d. Application.
Make a pile of dry flammable material such as rags, papers, empty boxes, or cartons. Spread out a piece of absorbent paper on this material. Spread igniter material on the absorbent paper and place the jar (on its side) on top of the igniter material. Make certain the jar does not leak. When the acid soaks through or corrodes the paper, it will contact the igniter material and cause it to burst into flame.
This device is not reliable at temperatures below 40° F. The time delay depends on the thickness of the paper. A similar device should be tested to determine the delay provided by various thicknesses of paper. It should be tested